Calorimeter
for screening synthesis reactions
A laboratory reactor
capable of simulating experimental industrial conditions and providing rapid access
to important thermodynamic properties of liquid-liquid and liquid-gas mixtures:
reaction heat, mixing heat, reaction time, maximum elevations of temperature
during reaction, monitoring of reaction kinetics, heat capacities, etc.
Used as a screening tool to determine reaction heats, the DRC offers numerous
advantages.
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DRC operating from -80 to 150C
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Atmospheric
pressure
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Calibration
by Joule effect
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Reactor
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double skinned flasks
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vol 100,250 or 500 ml
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material pyrex
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Stirrer
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anchor shape
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teflon
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speed from 50 to
1,000 rpm
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torque 30 N.cm
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Dosing system
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funnel
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volume 50 ml
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Probes
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tantalum sheathed
platinum probe 100W
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Joule effect probe
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pH-meter
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Cryo-thermostat
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temperature control
1.01C
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